Sinteza Ni, Co in Cu koordinacijskih spojin z derivati pirola

diplomsko delo

Mojca Dajčman (Author), Matjaž Kristl (Mentor), Mihael Drofenik (Co-mentor)

Abstract

V sklopu diplomskega dela sem sintetizirala 21 koordinacijskih spojina niklja, kobalta in bakra. Pri tem sem uporabila nikljev acetat tetrahidrat, kobaltov acetat tetrahidrat, bakrov acetat hidrat, ter štiri ligande, od tega tri v trdnem agregatnem stanju, to so pirazol, imidazol in 1,2,4-triazol, in enega v tekočem agregatnem stanju, pirolidin. Kot topila sem uporabila metanol, etanol in dietil eter. Za dobljene spojine sem opravila termogravimetrično analizo (TGA) in Fourierjevo transformacijsko infrardečo spektroskopijo (FTIR). Dobljene rezultate sem predstavila v tabelah.

Keywords

kemija;pirazol;imidazol;triazol;pirolidin;koordinacijske spojine;termogravimetrija;Fourierjeva spektroskopija;diplomska dela;

Data

Language:	Slovenian
Year of publishing:	2012
Source:	Maribor
Typology:	2.11 - Undergraduate Thesis
Organization:	UM FNM - Faculty of Natural Sciences and Mathematics
Publisher:	[M. Dajčman]
UDC:	54(043.2)
COBISS:	19572744
Views:	2107
Downloads:	166
Average score:	0 (0 votes)
Metadata:

Other data

Secondary language:	English
Secondary title:	Synthesis of Ni, Co and Cu coordination compounds whit derivatives of pirol
Secondary abstract:	As part of my diploma thesis I have synthesized twenty-one coordination compounds of nickel, cobalt and copper. For this I used nickel acetate tetrahydrate, cobalt acetate tetrahydrate, copper acetate hydrate and four ligands: pyrazole, imidazole and 1,2,4-triazole in the solid state and pyrrolidine in liquid state. As solvents I used methanol, ethanol and diethyl ether. I conducted thermogravimetric analysis (TGA) and Fourier transform infrared spectroscopy (FTIR). The results were presented in tables.
Secondary keywords:	pyrazole;imidazole;1;2;4-triazole;pyrrolidine;coordination compounds;thermogravimetric analysis (TGA);Fourier transformation infrared spectroscopy (FTIR);
URN:	URN:SI:UM:
Type (COBISS):	Undergraduate thesis
Thesis comment:	Univ. v Mariboru, Fak. za naravoslovje in matematiko, Oddelek za kemijo
Pages:	XIII, 66 f.
Keywords (UDC):	mathematics;natural sciences;naravoslovne vede;matematika;chemistry;crystallography;mineralogy;kemija;
ID:	1026956