diplomsko delo
Meta Colnar (Author), Iztok Turel (Mentor)

Abstract

V okviru diplomskega dela sem optimizirala sintezo organorutenijevega(II) kompleksa s piritionom in pta, katerega je v okviru svojega diplomskega dela sintetizirala že Tjaša Rijavec. S spreminjanjem reakcijskih pogojev sem želela čim bolj optimizirati sintezo ter tako izboljšati izkoristek reakcije, pri tem pa sem pazila na ohranjanje čistosti kompleksa. Menjala sem topilo, sol, spreminjala reakcijski čas sinteze, ekvivalente reagentov in izvajala sintezo pod različnimi temperaturnimi pogoji. Dobljene komplekse sem analizirala z elementno analizo in jedrsko magnetno resonanco ter tako preverjala ustreznost in čistost sintetiziranih spojin.

Keywords

rutenij;organorutenijevi(II) kompleksi;ligandi;pirition;pta;sinteza;optimizacija sinteze;diplomske naloge;

Data

Language: Slovenian
Year of publishing:
Typology: 2.11 - Undergraduate Thesis
Organization: UL FKKT - Faculty of Chemistry and Chemical Technology
Publisher: [M. Colnar]
UDC: 546.96:547.82(043.2)
COBISS: 1538308547 Link will open in a new window
Views: 641
Downloads: 126
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Other data

Secondary language: English
Secondary title: Optimization of the synthesis of organoruthenium (II) complex with pyrithion and pta
Secondary abstract: The purpose of my thesis was optimization of the synthesis of organoruthenium(II) complex with pyrithione and pta, which was firstly preparedby Tjaša Rijavec in her bachelor’s thesis. By changing various reaction conditions I wanted to obtain better yield of the pta complex as well as to achieve required purity. This was attained by using different solvents, salts, changing reaction time of the synthesis; equivalents of reagents and carrying synthesis under different temperature condition. Synthesised complexes were characterized and checked for the purity by nuclear magnetic resonance and elemental analysis.
Secondary keywords: optimization;organoruthenium(II) complex;pyrithione;pta;
Type (COBISS): Bachelor thesis/paper
Study programme: 1000374
Embargo end date (OpenAIRE): 1970-01-01
Thesis comment: Univ. v Ljubljani, Fak. za kemijo in kemijsko tehnologijo, VSŠ Kemijska tehnologija
Pages: 33 str.
ID: 11214253