diplomsko delo
Uroš Rapuš (Author), Jakob Kljun (Mentor)

Abstract

Namen diplomske naloge je bil pripraviti železove in bakrove koordinacijske spojine tiohidroksamskih kislin ter njihova karakterizacija. V okviru diplomske naloge sem sintetiziral in optimiziral sintezo dveh tiohidroksamskih kislin, ter pripravil komplekse tudi s tremi drugimi kislinami. Sintetizirane tiohidroksamske kisline sem okarakteriziral z jedrsko magnetno resonanco (NMR), masno spektrometrijo in IR spektroskopijo. Pripravljene koodinacijske spojine pa sem okarakteriziral z masno spektrometrijo, elementno analizo CHN, ter IR in UV-Vis spektroskopijo.

Keywords

bioanorganska kemija;koordinacijske spojine;železo;baker;ligandi;tiohidroksamske kisline;fluopsini;diplomska dela;

Data

Language: Slovenian
Year of publishing:
Typology: 2.11 - Undergraduate Thesis
Organization: UL FKKT - Faculty of Chemistry and Chemical Technology
Publisher: [U. Rapuš]
UDC: 546.56:546.72:547-327(043.2)
COBISS: 1538319555 Link will open in a new window
Views: 860
Downloads: 256
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Other data

Secondary language: English
Secondary abstract: The purpose of my thesis was to prepare and characterize iron and copper coordination compounds of thiohydroxamic acids. Two thiohydroxamic acids were prepared and their synthesis protocols were optimized. Complexes of said acids and complexes with three other acids were prepared. The synthesized acids were characterized with nuclear magnetic resonance (NMR), mass spectrometry and IR spectroscopy. Prepared coordination compounds were characterized with mass spectrometry, elemental analysis CHN, IR and UV-Vis spectroscopy.
Secondary keywords: thiohydroxamic acid;iron;copper;
Type (COBISS): Bachelor thesis/paper
Study programme: 1000373
Embargo end date (OpenAIRE): 1970-01-01
Thesis comment: Univ. v Ljubljani, Fak. za kemijo in kemijsko tehnologijo
Pages: 54 str.
ID: 11216364