diplomsko delo
Uroš Pavlin (Author), Janez Cerkovnik (Mentor)

Abstract

V diplomski nalogi sem se osredotočil na pripravo kleščastih kompleksov tipa NCN-M (M = Pt, Pd, Ni). Najprej sem pripravil kleščasti NCN ligand, nato pa je sledila sinteza kompleksa s Pt, Pd in Ni kot kovino. Uspešno sem pripravil kleščaste komplekse s platino in paladijem, vendar mi kleščastega kompleksa s paladijem ni uspelo izolirati. Nastale produkte sem analiziral z 1H NMR spektroskopijo in plinsko kromatografijo, sklopljeno z masnim detektorjem (GC-MS).

Keywords

organokovinska kemija;koordinacijske spojine;kleščasti kompleksi;kleščasti ligandi;PCP;NCN;platina;paladij;nikelj;diplomske naloge;

Data

Language: Slovenian
Year of publishing:
Typology: 2.11 - Undergraduate Thesis
Organization: UL FKKT - Faculty of Chemistry and Chemical Technology
Publisher: [U. Pavlin]
UDC: 547:546.74:546.9(043.2)
COBISS: 19038467 Link will open in a new window
Views: 665
Downloads: 149
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Other data

Secondary language: English
Secondary title: Preparation of pincer complexes
Secondary abstract: In this work the preparation of NCN-M (M = Pt, Pd, Ni) pincer ligands and pincer complexes is described. First, NCN pincer ligand was prepared, followed by the synthesis of the complexes with Pt, Pd, and Ni metal. Complexes of platinum and palladium were sucessfully synthesized, however palladium pincer complex was not isolated. Products were analyzed with 1H NMR sprectroscopy and GC-MS chromatography.
Secondary keywords: pincer ligands;pincer complexes;coordination compounds;platinum;nickel;palladium;
Type (COBISS): Bachelor thesis/paper
Study programme: 1000374
Thesis comment: Univ. v Ljubljani, Fak. za kemijo in kemijsko tehnologijo, VSŠ Kemijska tehnologija
Pages: 29 f.
ID: 11811517