diplomsko delo
Abstract
V diplomski nalogi sem se osredotočil na pripravo kleščastih kompleksov tipa NCN-M (M = Pt, Pd, Ni). Najprej sem pripravil kleščasti NCN ligand, nato pa je sledila sinteza kompleksa s Pt, Pd in Ni kot kovino. Uspešno sem pripravil kleščaste komplekse s platino in paladijem, vendar mi kleščastega kompleksa s paladijem ni uspelo izolirati. Nastale produkte sem analiziral z 1H NMR spektroskopijo in plinsko kromatografijo, sklopljeno z masnim detektorjem (GC-MS).
Keywords
organokovinska kemija;koordinacijske spojine;kleščasti kompleksi;kleščasti ligandi;PCP;NCN;platina;paladij;nikelj;diplomske naloge;
Data
Language: |
Slovenian |
Year of publishing: |
2020 |
Typology: |
2.11 - Undergraduate Thesis |
Organization: |
UL FKKT - Faculty of Chemistry and Chemical Technology |
Publisher: |
[U. Pavlin] |
UDC: |
547:546.74:546.9(043.2) |
COBISS: |
19038467
|
Views: |
665 |
Downloads: |
149 |
Average score: |
0 (0 votes) |
Metadata: |
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Other data
Secondary language: |
English |
Secondary title: |
Preparation of pincer complexes |
Secondary abstract: |
In this work the preparation of NCN-M (M = Pt, Pd, Ni) pincer ligands and pincer complexes is described. First, NCN pincer ligand was prepared, followed by the synthesis of the complexes with Pt, Pd, and Ni metal. Complexes of platinum and palladium were sucessfully synthesized, however palladium pincer complex was not isolated. Products were analyzed with 1H NMR sprectroscopy and GC-MS chromatography. |
Secondary keywords: |
pincer ligands;pincer complexes;coordination compounds;platinum;nickel;palladium; |
Type (COBISS): |
Bachelor thesis/paper |
Study programme: |
1000374 |
Thesis comment: |
Univ. v Ljubljani, Fak. za kemijo in kemijsko tehnologijo, VSŠ Kemijska tehnologija |
Pages: |
29 f. |
ID: |
11811517 |