Tvorba kokristalov organokovinskih spojin z jodom in jodovimi spojinami

diplomsko delo

Sabina Klemenc (Author), Franc Perdih (Mentor)

Abstract

V okviru diplomskega dela sem pripravila različne kokristale z jodom in jodovimi spojinami. Kokristale sem pripravila iz organokovinskih spojin in jodom oz. jodovih spojin v različnih stehiometričnih razmerjih. Reakcije sem izvedla ob dodatku topila in segrevanju, nato sem pustila zmesi stati na sobni temperaturi teden dni, pokrito s parafilmom, da sem dobila kristale primerne velikosti za nadaljno obdelavo. S pomočjo rentgenske praškovne analize smo posneli difraktograme in jih primerjali s simuliranimi difraktogrami.

Keywords

halogeni;halogenska vez;jod;jodove spojine;kokristali;rentgenska praškovna difrakcija;diplomske naloge;

Data

Language:	Slovenian
Year of publishing:	2021
Typology:	2.11 - Undergraduate Thesis
Organization:	UL FKKT - Faculty of Chemistry and Chemical Technology
Publisher:	[S. Klemenc]
UDC:	546.15:548(043.2)
COBISS:	89661699
Views:	182
Downloads:	21
Average score:	0 (0 votes)
Metadata:

Other data

Secondary language:	English
Secondary title:	Co-crystal formation of organometallic compounds with iodine and iodine compounds
Secondary abstract:	As part of my degree work, I prepared various cocrystals with iodine and iodine compounds. The starting materials were prepared from organometallic compounds and iodine or of iodine compounds in different stoichiometric ratios. The reactions were performed with the addition of solvent and under heating then the solutions stand on room temperature for one week, covered with parafilm, to obtain crystals of suitable size for further processing. Using X-ray powder analysis, diffractograms were recorded and compared with simulated diffractograms.
Secondary keywords:	cocrystals;iodine compounds;X-ray powder analysis;
Type (COBISS):	Bachelor thesis/paper
Study programme:	1000374
Thesis comment:	Univ. v Ljubljani, Fak. za kemijo in kemijsko tehnologijo, VSŠ Kemijska tehnologija
Pages:	34 f.
ID:	13961678