diplomsko delo
Benjamin Poljanc (Author), Iztok Turel (Mentor)

Abstract

Cilj diplomske naloge je bila optimizacija že znane sintezne poti za pripravo piritionov s trifluorometilno skupino in uporaba le-teh za sintezo cinkovih koordinacijskih spojin. Pri eksperimentalnem delu so bili sintetizirani štirje analogi piritiona s trifluorometilno skupin na različnih položajih aromatskega obroča, ki so bili nato uporabljeni kot ligandi za sintezo cinkovih koordinacijskih spojin. Sintetizirani piritioni in njihovi cinkovi kompleksi so bili karakterizirani z jedrsko magnetno resonanco (NMR) ter z UV-Vis in IR spektroskopijo. Pripravljeni piritioni so bili dodatno karakterizirani tudi z masno spektrometrijo.

Keywords

derivati piridina;substituirani piritioni;fluor;cink;cinkovi kompleksi;ligandi;optimizacija;diplomska dela;

Data

Language: Slovenian
Year of publishing:
Typology: 2.11 - Undergraduate Thesis
Organization: UL FKKT - Faculty of Chemistry and Chemical Technology
Publisher: [B. Poljanc]
UDC: 547.82:546.47(043.2)
COBISS: 126254595 Link will open in a new window
Views: 35
Downloads: 17
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Other data

Secondary language: English
Secondary title: Optimisation of synthesis of selected pyrithione derivatives and preparation of their coordination compounds with zinc
Secondary abstract: The aim of my work was to optimize an already known synthetic route of pyrithiones with trifluoromethyl group and to prepare their coordination compounds with zinc. Four different pyrithione analogues with different positions of the trifluoromethyl group on the aromatic ring were synthesized and later used as ligands for the preparation of zinc complexes. The synthesized pyrithiones and their zinc complexes were characterized by nuclear magnetic resonance (NMR), UV-Vis and IR spectroscopy. The pyrithiones were also characterized by mass spectrometry.
Secondary keywords: optimisation;substituted pyrithiones;fluoruine;zinc;Univerzitetna in visokošolska dela;
Type (COBISS): Bachelor thesis/paper
Study programme: 1000373
Embargo end date (OpenAIRE): 1970-01-01
Thesis comment: Univ. v Ljubljani, Fak. za kemijo in kemijsko tehnologijo, UNI Kemija
Pages: 55 str.
ID: 16382222