Sinteza kelatnih analogov halicina
diplomsko delo
Abstract
Halicin je spojina, ki je sestavljena iz dveh heterocikličnih obročev, ki ju povezuje žveplov atom. V okviru diplomskega dela sem pripravila različne spojine podobne halicinu, v katerih sem spreminjala heterociklične substituente. Cilj raziskovalnega dela je bil optimizirati izkoristek reakcij in odstraniti prisotne nečistoče. Spojine sem karakterizirala z jedrsko magnetno resonanco, elementno analizo in masno spektrometrijo visoke ločljivosti. Kristali so bili karakterizirani z rentgensko strukturno analizo. Rezultati karakterizacij so pri nekaterih sintezah pokazali uspešno sintetiziran produkt.
Keywords
halicin;piridini;tiofenol;sinteza;fizikalno-kemijska karakterizacija;diplomske naloge;
Data
| Language: | Slovenian |
|---|---|
| Year of publishing: | 2022 |
| Typology: | 2.11 - Undergraduate Thesis |
| Organization: | UL FKKT - Faculty of Chemistry and Chemical Technology |
| Publisher: | [T. Krajnc] |
| UDC: | 547.82.057(043.2) |
| COBISS: |
128819203
|
| Views: | 69 |
| Downloads: | 14 |
| Average score: | 0 (0 votes) |
| Metadata: |
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Other data
| Secondary language: | English |
|---|---|
| Secondary title: | Synthesis of chelating analogs of halicin |
| Secondary abstract: | Halicin is a compound in which two heterocycles are connected by a sulfur atom. In the framework of the diploma thesis, I prepared different compounds similar to halicin in which I varied heterocyclic substituents. The goal of the research was to optimise the yield of reactions and to remove any impurities present. The compounds were characterized with nuclear magnetic resonance, elemental analysis and mass spectrometry of high resolution. The crystals were characterized by X-ray structural analysis. The results of characterizations have shown a successfully synthetised product in some syntheses. |
| Secondary keywords: | halicin;synthesis;physico-chemical characterization;Heterociklične spojine;Univerzitetna in visokošolska dela; |
| Type (COBISS): | Bachelor thesis/paper |
| Study programme: | 1000374 |
| Embargo end date (OpenAIRE): | 1970-01-01 |
| Thesis comment: | Univ. v Ljubljani, Fak. za kemijo in kemijsko tehnologijo, VSŠ Kemijska tehnologija |
| Pages: | 40 str. |
| ID: | 16411113 |
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