diplomsko delo
Jan Polak (Author), Iztok Turel (Mentor)

Abstract

Namen diplomske naloge je bil sintetizirati koordinacijske spojine niklja(II) s triflourometil substituiranimi piritioni. Piritione sem sintetiziral dvostopenjsko iz 2-kloro piridinov. Pripravljene produkte sem uporabil kot ligande za sintezo nikljevih koordinacijskih spojin. Vse nastale spojine sem karakteriziral z jedrsko magnetno resonanco (NMR), IR spektroskopijo, UV-Vis spektroskopijo, CHN elementno analizo in masno spektroskopijo visoke ločljivosti (HRMS). Iz določenih spojin sem pripravil monokristale, ki so bili analizirani z rentgensko difrakcijo (XRD).

Keywords

ligandi;pirition;sinteza ligandov;sinteza koordinacijskih spojin;karakterizacija;diplomska dela;

Data

Language: Slovenian
Year of publishing:
Typology: 2.11 - Undergraduate Thesis
Organization: UL FKKT - Faculty of Chemistry and Chemical Technology
Publisher: [J. Polak]
UDC: 546.74:547.82(043.2)
COBISS: 207265283 Link will open in a new window
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Downloads: 15
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Other data

Secondary language: English
Secondary title: Synthesis of nickel coordination compounds with selected pyrithiones
Secondary abstract: The purpose of my thesis was to synthesize nickel coordination compounds with trifuoromethyl substituted pyrithiones. I synthesized the pyrithiones in two steps from 2-chloro pyridines. I used the prepared products as ligands for the formation of nickel coordination compounds. I characterized the resulting compounds with nuclear magnetic resonance (NMR), IR spectroscopy, UV-Vis spectroscopy, CHN elemental analysis and high resolution mass spectroscopy (HRMS). I obtained single crystals of certain compounds, which were analysed with X-ray diffraction (XRD).
Secondary keywords: pyrithione;nickel;synthesis;characterization;Bioanorganska kemija;Koordinacijske spojine;Nikelj;Univerzitetna in visokošolska dela;
Type (COBISS): Bachelor thesis/paper
Study programme: 1000373
Embargo end date (OpenAIRE): 1970-01-01
Thesis comment: Univ. v Ljubljani, Fak. za kemijo in kemijsko tehnologijo, UNI Kemija
Pages: 1 spletni vir (1 datoteka PDF (48 str.))
ID: 24956292