Irena Ban (Author), Matjaž Kristl (Author), Mihael Drofenik (Author), Arkadije Popović (Author)

Abstract

A new hydroxylammonium compound (NH3OH)2GeF6, has been synthesized by the addition of solid NH3OHF to a solution of GeO2 dissolved in 20% HF. The compound was characterized by chemical analysis and X-ray powder diffraction, the thermal decomposition was studied by thermal analysis and mass spectrometry. (NH3OH)2GeF6 crystallizes monoclinic. Two endothermic and two exothermic peaks have been observed on the DSC curve, the decomposition product at 500 °C is GeO2.

Keywords

anorganska kemija;sinteze;karakterizacija;hidroksilamonijevi fluorogermanati;rentgenska praškovna analiza;masna spektroskopija;termična analiza;inorganic chemistry;synthesis;characterisation;hydroxylammonium fluorogermanates;x-ray powder diffraction;mass spectroscopy;thermal analysis;

Data

Language: English
Year of publishing:
Typology: 1.01 - Original Scientific Article
Organization: UM FKKT - Faculty of Chemistry and Chemical Engineering
UDC: 541.49.057:548.73
COBISS: 8703766 Link will open in a new window
ISSN: 0040-6031
Views: 2043
Downloads: 89
Average score: 0 (0 votes)
Metadata: JSON JSON-RDF JSON-LD TURTLE N-TRIPLES XML RDFA MICRODATA DC-XML DC-RDF RDF

Other data

Secondary language: English
Secondary keywords: anorganska kemija;sinteze;karakterizacija;hidroksilamonijevi fluorogermanati;rentgenska praškovna analiza;masna spektroskopija;termična analiza;
URN: URN:SI:UM:
Pages: str. 253-257
Volume: ǂVol. ǂ419
Issue: ǂiss. ǂ1/2
Chronology: 2004
ID: 8718694
Recommended works:
, no subtitle data available
, synthesis and characterisation of a new fluorovanadate
, diplomsko delo univerzitetnega študijskega programa
, diplomsko delo univerzitetnega študijskega programa
, diplomsko delo visokošolskega strokovnega študijskega programa I. stopnje