Hydroxylammonium fluorogermanates
Abstract
A new hydroxylammonium compound (NH3OH)2GeF6, has been synthesized by the addition of solid NH3OHF to a solution of GeO2 dissolved in 20% HF. The compound was characterized by chemical analysis and X-ray powder diffraction, the thermal decomposition was studied by thermal analysis and mass spectrometry. (NH3OH)2GeF6 crystallizes monoclinic. Two endothermic and two exothermic peaks have been observed on the DSC curve, the decomposition product at 500 °C is GeO2.
Keywords
anorganska kemija;sinteze;karakterizacija;hidroksilamonijevi fluorogermanati;rentgenska praškovna analiza;masna spektroskopija;termična analiza;inorganic chemistry;synthesis;characterisation;hydroxylammonium fluorogermanates;x-ray powder diffraction;mass spectroscopy;thermal analysis;
Data
| Language: | English |
|---|---|
| Year of publishing: | 2004 |
| Typology: | 1.01 - Original Scientific Article |
| Organization: | UM FKKT - Faculty of Chemistry and Chemical Engineering |
| UDC: | 541.49.057:548.73 |
| COBISS: |
8703766
|
| ISSN: | 0040-6031 |
| Views: | 2043 |
| Downloads: | 89 |
| Average score: | 0 (0 votes) |
| Metadata: |
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Other data
| Secondary language: | English |
|---|---|
| Secondary keywords: | anorganska kemija;sinteze;karakterizacija;hidroksilamonijevi fluorogermanati;rentgenska praškovna analiza;masna spektroskopija;termična analiza; |
| URN: | URN:SI:UM: |
| Pages: | str. 253-257 |
| Volume: | ǂVol. ǂ419 |
| Issue: | ǂiss. ǂ1/2 |
| Chronology: | 2004 |
| ID: | 8718694 |
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