diplomsko delo univerzitetnega študijskega programa
Abstract
Koordinacijske spojine so dandanes pogosto sintetizirane in imajo širok spekter uporabnosti. Namen raziskave je bil sintetizirati nove in že znane koordinacijske spojine z bakrom, kobaltom in nikljem. V sklopu diplomskega dela smo izvedli 27 reakcij sinteze koordinacijskih spojin z bakrom, kobaltom in nikljem ter ligandi nikotinsko, izonikotinsko in pikolinsko kislino. Kot topila smo uporabili vodo, N,N-dimetilformamid in mešanico metanola in acetonitrila. Produkte sintez smo nato analizirali z rentgensko praškovno difrakcijo in termogravimetrično analizo.
Keywords
koordinacijske spojine;kobalt;baker;nikotinska kislina;izonikotinska kislina;pikolinska kislina;rentgenska praškovna difrakcija;termogravimetrična analiza;TGA;
Data
Language: |
Slovenian |
Year of publishing: |
2013 |
Typology: |
2.11 - Undergraduate Thesis |
Organization: |
UM FKKT - Faculty of Chemistry and Chemical Engineering |
Publisher: |
[L. Goljat] |
UDC: |
56.562.022:543.427(043.2) |
COBISS: |
17486870
|
Views: |
1954 |
Downloads: |
198 |
Average score: |
0 (0 votes) |
Metadata: |
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Other data
Secondary language: |
English |
Secondary title: |
Synthesis of copper, nickel and cobalt coordination compounds with nicotinic, isonicotinic and picolinic acid |
Secondary abstract: |
Coordination compounds are nowadays often synthesized and have a wide range of uses. The purpose of this study was to synthesize new and already known coordination compounds with copper, cobalt and nickel. As part of the thesis we performed 27 synthesis of coordination compounds with copper, cobalt, nickel and Iigands nicotinic, isonicotinic and picolinic acid. As solvents, we used water, N, N-Dimethylformamide, and a mixture of methanol and acetonitrile. Synthesis products were analyzed by X-ray diffraction and thermogravimetric analysis. |
Secondary keywords: |
coordination compounds;cobalt;cooper;nickel;nicotinic acid;isonicotinic acid;X-ray diffraction;thermogravimetric analysis; |
URN: |
URN:SI:UM: |
Type (COBISS): |
Undergraduate thesis |
Thesis comment: |
Univ. v Mariboru, Fak. za kemijo in kemijsko tehnologijo |
Pages: |
XIV, 85 f. |
ID: |
8727384 |