Uporaba sonokemijske metode v sintezi bakrovih metanoatov

diplomsko delo univerzitetnega študijskega programa I. stopnje

Mateja Biškop (Author), Matjaž Kristl (Mentor), Irena Ban (Co-mentor)

Abstract

Sonokemija je področje kemije, kjer kemijske reakcije potekajo pod vplivom zvočne energije, imenovane ultrazvok. Ukvarja se z razumevanjem učinka zvočnih valov na kemijske sisteme. Namen naše diplomske naloge je bil sintetizirati različne modifikacije bakrovih metanoatov z uporabo klasičnih metod kot tudi z metodami sonokemije. V sklopu diplomske naloge smo vzorce bakrovih metanoatov najprej sintetizirali, kasneje pa smo jih analizirali s pomočjo rentgenske praškovne difrakcije (XRD) in termogravimetrične analize (TGA). Našo predpostavljeno hipotezo smo potrdili, saj nam je uspelo sintetizirati različne modifikacije bakrovih metanoatov s spreminjanjem parametrov, kot so volumen in koncentracija mravljične kisline ter masa bazičnega bakrovega karbonata, ki sta služili kot vstopni spojini.

Keywords

baker;koordinacijske spojine;bakrovi metanoati;sonokemija;rentgenska praškovna difrakcija;termogravimetrična analiza;

Data

Language:	Slovenian
Year of publishing:	2015
Typology:	2.11 - Undergraduate Thesis
Organization:	UM FKKT - Faculty of Chemistry and Chemical Engineering
Publisher:	[M. Biškop]
UDC:	544.57(043.2)
COBISS:	19428374
Views:	1201
Downloads:	60
Average score:	0 (0 votes)
Metadata:

Other data

Secondary language:	English
Secondary title:	APPLICATION OF SONOCHEMICAL METHOD IN THE SYNTHESIS OF COPPER METANOATES
Secondary abstract:	Sonochemistry is the field od chemistry, where chemical reactions take place under the infulence of sound energy, called ultrasound. It deals with understanding of the effect of sound waves in chemical systems. The aim of our study was to synthesize various modifications of copper methanoates using not only classical methods but also methods of sonochemistry. Within the thesis, samples of copper methanoates were first synthesized and subsequently analysed using X-ray powder diffraction (XRD) and thermogravimetric analysis (TGA). Our assumed hypothesis was confirmed, because we have managed to synthesize various modifications of copper methanoates by varying parameters such as volume and concentration of formic acid as well as mass of basic copper carbonate, which were used as the input compounds.
Secondary keywords:	cooper;coordination compounds;cooper formates;sonochemistry;X-ray powder diffraction;thermogravimetric analysis;
URN:	URN:SI:UM:
Type (COBISS):	Bachelor thesis/paper
Thesis comment:	Univ. v Mariboru, Fak. za kemijo in kemijsko tehnologijo
Pages:	IX, 53 f.
ID:	8887541